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Coupling information is very useful in locating the position of an atom in relation to other atoms. This puzzle covers one such example. For an unknown compound1, the 13C assignment is not clear for carbons 116 or 134 ppm. The 13C NMR spectrum shows the 19F-13C coupling for the carbon at 116 ppm as 23.7...

Takeda has invested significant time and effort in digitalizing and automating R&D. In synthetic molecule process development (SMPD) this involved building up high-throughput experimentation (HTE) and automation capabilities to accelerate process optimization. Join Adrian Ramirez Galilea, Associate Director of Automation & HTE at Takeda, as he shares his experience and insights. He will discuss: How...

What’s That Peak? Structure Elucidation & Verification Virtual Symposium What’s in my sample? Did I make what I think I made? What’s that peak? Questions that are answered by structure elucidation and & verification are integral parts of chemical R&D workflows from discovery to development and manufacturing. But as scientists constantly strive to do their...

Optimization of chemical process development means exploring complex parameter spaces. Traditional manual approaches are time-consuming, tedious and low throughput. Discover the next generation of AI-driven, digitalized design, make, test, analyze (DMTA) cycles in pharmaceutical R&D with ACD/Labs and Atinary SDLabs™ platform.